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1 article(s) from Hardy, Matthias

A heterobimetallic tetrahedron from a linear platinum(II)-bis(acetylide) metalloligand

Matthias Hardy,
Marianne Engeser and
Arne Lützen

Beilstein J. Org. Chem. 2020, 16, 2701–2708, doi:10.3762/bjoc.16.220

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Scheme 1: Stepwise assembly of the heterobimetallic tetrahedron 4, starting from 4-ethynylaniline (1) and tra...

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Figure 1: ESI(+) mass spectrum of heterobimetallic complex 4. The top inset shows the experimentally observed...

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Figure 2: UV–vis spectrum of heterobimetallic complex 4 (1150 µM in acetonitrile at 295 K, 0.01 mm cuvette).

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Figure 3: Schematic representation of symmetry-considerations concerning possible diastereomeric tetrahedra. ...

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Figure 4: Detailed excerpt of the ³¹P NMR spectrum of 4 (202 MHz, acetonitrile-d₃, 298 K).

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Figure 5: ¹H NMR and DOSY spectrum of heterobimetallic assembly 4 (500 MHz, acetonitilre-d₃, 298 K).

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Figure 6: GFN2-xTB minimized gas phase models of the cationic units of all possible diastereomers of 4. Color...

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Published 03 Nov 2020

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